Methods of Air Sampling and Analysis, 3rd Edition

Includes precise directions for a long list of contaminants! All contaminants you can analyze or monitor with a given method are consolidated together to facilitate use. This book is especially valuable for indoor and outdoor air pollution control, industrial hygiene, occupational health, analytical chemists, engineers, health physicists, biologists, toxicologists, and instrument users.

Preface
Publisher's Preface
Committees
Permissions

Part I : General Techniques
1 : Physical Precautions
2 : Calibration Procedures
3 : Dynamic Calibration of Air Analysis Systems with Permeation Tubes
4 : Sampling and Storage of Particles
5 : Sampling and Storage of Gases and Vapors
6 : Use and Care of Volumetric Glassware
7 : Reagent Water
8 : Common Acid, Alkali, and Other Standard Solutions
9 : Recovery and Internal Standard Procedures
10 : Interferences
11 : Terms and Symbols Relating to Molecular Spectroscopy
12 : Photometric Methods for Chemical Analysis
13 : Ultraviolet Absorption Spectroscopy
14 : Infrared Absorption Spectroscopy
15 : Atomic Absorption Spectroscopy
16 : Inductively Coupled Plasma Emission Spectroscopy
17 : Gas Chromatrography
18 : Radioactivity Analysis
19 : Precision and Accuracy
20 : General Safety Practices
21 : Air Purification
22 : Liquid Chromatography
23 : Thin-Layer Chromatography
24 : Instrumental Neutron Activation Analysis of Atmospheric Particulate Matter
25 : Use of Selective Ion Electrodes to Determine Air Pollutant Species
26 : Quality Control for Sampling and Analysis
27 : Direct Reading Colorimetric Indicators
28 : Fluorescence Spectrophotometry
29 : Sampling Aerosols by Filtration
30 : X-Ray Powder Diffraction
31 : X-Ray Fluorescence Analysis
32 : Chemiluminescent Analyzers
33 : Anodic Stripping Voltammetry (ASV)
34 : Ion Chromatography

Part II : Methods for Ambient Air Sampling and Analysis

100 : Carbon Compounds
A : Hydrocarbons
101 : Determinations of C1 Through C5 Atmospheric Hydrocarbons
102 : Separation and Determination of Polynuclear Aromatic Hydrocarbons and Benzo[a]pyrene
102A : Extraction and Cleanup Procedures for Polynuclear Aromatic Hydrocarbons in Atmospheric Particulate Matter
102B : Separation and Microanalysis of Airborne Particulate Matter for Benzo[a]pyrene Using Thin Layer Chromatography and Spectrofluorimetry
102C : Measurement of Benzo[a]pyrene and Benzo[k]fluoranthene by Spectrofluorimetry
102D : Measurement of Polynuclear Aromatic Hydrocarbons Using Liquid Chromatograhy with Fluorescence Detection
108 : Continuous Determination of Total Hydrocarbons in the Atmosphere (Flame Ionization Method)
109 : Flame Ionization Detector

B : Related Organic Compounds
114 : Determination of Acrolein Content of the Atmosphere (Colorimetric)
116 : Determination of Formaldehyde Content of the Atmosphere (Colorimetric Method)
117 : Determination of Formaldehyde Content of the Atmosphere (MBTH Colorimetric Method - Application to Other Aldeydes)
118 : Determination of Mercaptan Content of the Atmosphere
121 : Determination of Phenols in the Atmosphere (Gas Chromatographic Method)
122 : Determination of C1-C5 Aldehydes in Ambient Air and Source Emissions as 2,4-Dinitrophenylhydrazones by HPLC

C : Carbon Monoxide, Gas Analysis
128 : Determination of Continuous Carbon Monoxide Content of the Atmosphere (Nondispersive Infrared Method)
133 : Determination of O2, N2, CO, CO2, and CH4 (Gas Chromatographic Method)
134 : Constant Pressure Volumetric Gas Analysis for Oxygen, Carbon Dioxide, Carbon Monoxide, and Nitrogen (Orsat)
135 : Determination of Volatile Organic Compounds in Architectural and Industrial Surface Coatings

200 : Halogen and Halogen Compounds

201 : Chloride Content of the Atmosphere
202 : Determination of Free Chlorine Content of the Atmosphere (Methyl Orange Method)
203 : Determination of Fluoride Content of the Atmosphere and Plant Tissues (Manual Methods)
204 : Determination of Fluoride Content of the Atmosphere and Plant Tissue (Semiautomated Method)
205 : Determination of Fluoride Content of Plant Tissues (Potentiometric Method)
206 : Determination of Gaseous and Particulate Fluorides in the Atmosphere (Separation and Collection with Sodium Bicarbonate Coated Glass Tube and Particulate Filter)
207 : Determination of Gaseous and Particulate Fluorides in the Atmosphere (Separation and Collection with a Double Paper Tape Sampler)

300 : Metals

301 : Determination of Particulate Antimony Content of the Atmosphere
302 : Determination of Arsenic Content of Atmospheric Particulate Matter
303A : General Method for the Preparation of Non-Tissue Environmental Samples for Trace Metal Analysis
311-322 : Determination of a Number of Metals in Atmospheric Particulate Matter
317 : Determination of Elemental Mercury in Ambient and Workroom Air by Collection on Silver Wool and Atomic Absorption Spectroscopy
319 : Determination of Molybdenum Content of Atmospheric Particulate Matter by Atomic Absorption Spectrophotometry

400 : Inorganic Nitrogen Compounds and Oxidants

401 : Determination of Ammonia in the Atmosphere (Indophenol Method)
404 : Determination of Nitrate in Atmosphere Particulate Matter (Brucine Method)
405 : Determination of Nitric Oxide Content of the Atmosphere
406 : Determination of Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)
407 : Determination of Total Nitrogen Oxides as Nitrate (Phenoldisulphonic Acid Method)
408 : Analysis for Atmospheric Nitrogen Dioxide (24-H Average)
411 : Determination of Oxidizing Substances in the Atmosphere
413 : Determination of Ozone in the Atmosphere by Gas-Phase Chemiluminescence Instruments
415 : Determination of Atmospheric Nitric Acid
416 : Continuous Monitoring of Atmospheric Nitric Oxide and Nitrogen Dioxide by Chemiluminescence
417 : Continuous Monitoring of Ozone in the Atmosphere by Ultraviolet Photometric Instruments

500 : Particulate Matter

501 : High Volume Measurement of Size Classified Particulate Matter
502 : Particle Fallout Container Measurement of Dustfall from the Atmosphere
503 : Continuous Tape Sampling of Coefficient of Haze
507 : Integrating Nephelometer Measurement of Scattering Coefficient and Fine Particle Concentrations

600 : Radioactivity

601 : Determination of Gross Alpha Radioactivity Content of the Atmosphere
602 : Determination of Gross Beta Radioactivity Content of the Atmosphere
603 : Determination of the Iodine-131 Content of the Atmosphere (Particulate Filter Charcoal Gamma)
606 : Determination of Radon-222 Content of the Atmosphere
609A : Determination of Tritium Content of Water Vapor in the Atmosphere
609B : Determination of Elemental Tritium Content of the Atmosphere

700 : Sulfur Compounds

701 : Determination of Hydrogen Sulfide Content of the Atmosphere
704A : Determination of Sulfur Dioxide Content of the Atmosphere (Tetrachloromercurate Absorber/Parasaniline Method)
704B : Determination of Sulfur Dioxide Content of the Atmosphere (Formaldehyde Absorber/Pararosaniline Method)
704C : Determination of Sulfur Dioxide Content of the Atmosphere (Hydrogen Peroxide Method)
707 : Continuous Monitoring of Atmospheric Sulfur Dioxide with Amperometric Instruments
708 : Determination of Mercaptan Content of the Atmosphere
709 : Determination of Sulfur-Containing Gases in the Atmosphere (Continuous Method with Flame Photometric Detector)
709A : Determination of Sulfur-Containing Gases in the Atmosphere (Following Chromatographic mSeparation, with the FPD)
709B : Determination of Sulfur-Containing Gases in teh Atmosphere (Total Gaseous Sulfur with the FPD)
711 : Determination of Gaseous Sulfuric Acid and Sulfur Dioxide in Stack Gases
713 : Semi-Continuous Determination of Atmospheric Pariculate Sulfur, Sulfuric Acid and Ammonium Sulfates
714 : Determination of Sulfur Dioxide Emissions in Stack Gases by Pulsed Fluorescence
720A : Suppressed Anion Chromatography
720B : Nonsuppressed Anion Chromatography
720C : Flow Injection Determination of Aqueous Sulfate (Methylthymol Blue Method)
720D : Barium Sulfate Turbidimetry
720E : Barium Perchlorate Microtitration
720F : Barium Chloranilate Spectrophotometry
730 : Determination of Sulfur in Particulate Material by X-Ray Fluorescence

Part III : Methods for Chemicals in Air of the Workplace and in Biological Samples
800 : Methods for Chemicals in Air of the Workplace and in Biological Samples

801 : Determination of Ammonia in Air
804 : As, Se, and Sb in Urine and Air by Hydride Generation and Atomic Absorption Spectrometry
805 : Determination of Chloride in Air
806 : Determination of Free Chlorine in Air
807 : Determination of Chromic Acid Mist in Air
808 : Determination of Cyanide in Air
809 : Determination of Fluorides and Hydrogen Fluoride in Air
810 : Determination of Gaseous and Particulate Fluorides in Air
811 : Determination of Fluoride in Urine
812 : Determination of Hydrogen Sulfide in Air
815 : Determination of Mercury in Urine
816 : Determination of Nitric Oxide in Air
817 : Determination of Nitrogen Dioxide in Air
818 : Determination of Nitrogen Dioxide in Air
819 : Determination of Ozone in Air
821 : Determination of Phosgene in Air
822 : General Atomic Absorption Procedure for Trace Metals in Airborne Material Collected on Filters
822A : General Method for Preparation of Tissue Samples for Analysis for Trace Metals
822B : X-Ray Fluorescence Spectrometry for Multielement Analysis of Airborne Particulate and Biological Material
824 : Determination of Airborne Sulfates
825 : Determination of Acrolein in Air
826 : Determination of Acrolein in Air
827 : Determination of Aromatic Amines in Air
828 : Determination of Bis-(Chloromethyl) Ether (Bis-CME) in Air
829 : Determination of Chloromethyl Methyl Ether (CMME) and Bis-Chloromethyl Ehter (Bis-CME) in Air
830 : Determination of 3,3'-Dichloro-4,4'-Diaminodiphenylmethane (MOCA) in Air
831 : Determination of p,p-Diphenylmethane Diisocynate (MDI) in Air
832 : Determination of Nitroglycerin and Ethylene Glycol Dinitrate (Nitroglycol) in Air
833 : Determination of N-Nitrosodimethylamine in Ambient Air
834 : Determination of Organic Solvent Vapors in Air
835 : Determination of EPN, Malathion and Parathion in Air
836 : Determination of Total Particulate Aromatic Hydrocarbons (TpAH) in Air : Ultrasonic Extraction Method
837 : Determination of 2,4-Toluenediisocynate (TDI) in Air

Part IV : State-Of-The-Art Reviews

1 : The Measurement of Strong Acids in Atmospheric Samples
2 : Determination and Speciation of Ambient Particulate Sulfur Compounds
3 : Source Sampling for Regulated Air Pollutants from Stationary Sources

Part V : Conversion Factors

Index

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